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An Advanced Practical Course in NMR Techniques for Membrane Proteins

 

Rutherford Appleton Laboratory

11th - 14th May, 2009

 

 

Lectures:

 

Anja Böckmann             1.  Deuteration for solution and solid state NMR.

                                      2.  Aspects of protein assignment strategies and structure calculation.

 

Clemens Glaubitz          To be announced.

 

Victoria A. Higman        1.  Protein assignment, experiment types, labelling strategies, data management of large membrane systems using solid-state MAS NMR.

                                      2.  CCPNmr Analysis software and its use for assignment.

 

David Middleton            1.  Methods of rendering proteins into a form for high resolution solid state NMR.

                                      2.  Small molecule studies of membrane receptors.

 

Alain Milon                   1.  Labeling strategies and structural resolution of beta-barrel porins by solution state NMR:  A. Milon

                                      2.  Structural resolution of beta barrel porins by solution state NMR: practical based on real experimental NMR spectra, assignment, restrained molecular dynamics:  M. Renault,

                                     

Niels Nielsen                 1.  Using SIMPSON.

                                      2.  Solid state NMR theory and pulse sequence for membrane protein analysis.

 

Hartmut Oschkinat         1.  Successes of solid state NMR in resolving structures of membrane proteins and dynamical complexes

 

 

 

 

Practical demonstrations:

 

Anja Böckmann             Protocols how to achieve high degrees of deuteration for proteins.

 

Clemens Glaubitz          To be announced.

 

Victoria A. Higman        Solution and solid-state MAS NMR data collection/instrument set up and structure calculations / restraint generation.

 

Alain Milon                   MACADAM for membrane peptides.

 

David Middleton            Tips on how to make nanocrystals, amorphous and lyophilized samples for high resolution solid state NMR studies.

 

Niels Nielsen                 Use of SIMPSON.

 

Hartmut Oschkinat         To be announced

 

 

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